HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pyrrolidineethanamine → HCID 59851410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pyrrolidineethanamine | HCID 1344 | — |
| Reactant | HCID 59852114 | HCID 59852114 | — |
| Product | HCID 59851410 | HCID 59851410 | — |
Reaction Steps
In a manner similar to that described for Method N, 2-(3,4-dimethoxy-phenylamino)-6-oxo-6,7-dihydro-5H-benzo[b]pyrimido[4,5-d]azepine-10-carboxylic acid (I-43) and 2-(pyrrolidin-1-yl)ethanamine were converted to I-75 (6%) after purification by C-18 RP LC-MS chromatography. HRMS Calcd. for C27H11N6O4: 503.2406, Found 503.2399.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935694B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-ceaaa3f25dd546a7ac523dd5b11f21e1 |
| Source note | uspto-grants-2011_05 |