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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 545014Generated: October 27, 2026

8-chloro-4-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dione → HCID 59851075, compound

https://huagongshe.com/reaction/545014

Reaction equation

Participants

RoleNameHCIDCharge
Reactant8-chloro-4-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dioneHCID 66934877—
ReactantHCID 178512500HCID 178512500—
ProductHCID 59851075HCID 59851075—

Reaction Steps

In a manner similar to that described for method I, 8-chloro-4-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-j) and 1-(4-chlorophenyl)guanidine were converted to I-11 (23%): HRMS Calcd. for C18H12Cl2N4O: 371.0466, Found 371.0471.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07935694B2
Source datasetuspto-grants-2011_05
ORD IDord-4fef688a6e0b4445bb53b8ab0a3057ca
Source noteuspto-grants-2011_05