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HRID545020

反应详情

EQUATION

反应方程式

HRID 545020 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=N)N.O=S(=O)(O)O
HCID220673

Sulfuric acid--N,N-dimethylguanidine (1/1)

C3H11N3O4S

结构：CN(C)C=C1CC(=O)Nc2cc(Cl)ccc2C1=O
HCID66934877

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1ncc2c(n1)-c1ccc(Cl)cc1NC(=O)C2
HCID59852003

未命名化合物

PROCEDURE

实验过程

In a manner similar to that described for method I, 8-chloro-4-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-j) and 1,1-dimethylguanidine sulfate were converted to I-22 (42%): HRMS Calcd. for C14H13ClN4O: 289.0856, Found 289.0843.