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HRID545031

反应详情

EQUATION

反应方程式

HRID 545031 的结构方程式

REACTANTS

反应物

2
结构：C#CCN1CCCC1
HCID299616

1-(prop-2-yn-1-yl)pyrrolidine

C7H11N

结构：O=C1Cc2cnc(Nc3ccc(I)cc3)nc2-c2ccc(Cl)cc2N1
HCID56946588

未命名化合物

PRODUCTS

生成物

1
结构：O=C1Cc2cnc(Nc3ccc(C#CCN4CCCC4)cc3)nc2-c2ccc(Cl)cc2N1
HCID59851312

未命名化合物

PROCEDURE

实验过程

In a manner similar to that described for Method O, 9-chloro-2-(4-iodo-phenylamino)-5H,7H-benzo[b]pyrimido[4,5-d]azepin-6-one (I-36) and 1-(prop-2-ynyl)pyrrolidine were converted to I-47 (52%): HRMS Calcd. for C25H22ClN5O: 444.1591, Found 444.1589.