反应详情

To a solution of 10 g (0.18 mol) of cyclopropylamine in 50 ml of EtOH was added 7 g (0.04 mol) of ethylbromoacetate and the reaction stirred for 1 h. The reaction was then evaporated to dryness, redissolved in CH2Cl2 washed with water, dried over sodium sulfate and concentrated to afford 6 g (quant.) of the title compound as a colorless oil. MS: 144.1 (MH+).

1. customThe reaction was then evaporated to dryness
2. dissolutionredissolved in CH2Cl2
3. washwashed with water
4. dry with materialdried over sodium sulfate
5. concentrationconcentrated