HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-benzyl-1-phenylethylamine → N-benzyl-1-phenylethanimine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-benzyl-1-phenylethylamine | HCID 519427 | — |
| Reactant | Acetic anhydride pyridine | HCID 22348678 | — |
| Product | N-benzyl-1-phenylethanimine | HCID 297338 | — |
Reaction Steps
Benzyl-(1-phenylethyl)amine, conversion>99%, ee 82% (GC, sample derivatised by treatment with acetic anhydride pyridine, Chirasil DEX CB, 25 m×0.25 mm, injector/detector 200° C., helium 20 psi, 170° C. for 40 minutes then ramp at 15° C./min to 200° C., retention times 29.71 minutes and 30.73 minutes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935841B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-13ba5d3ba5294e9b950de64a67b4ef6c |
| Source note | uspto-grants-2011_05 |