HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 23712812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 17842376 | HCID 17842376 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23712812 | HCID 23712812 | 107.6% |
Reaction Steps
Water (6.0 ml) and lithium hydroxide (99.7 mg) were added to a solution of 2-methoxycarbonyl-5-methyl-4,5,6,7-tetrahydrooxazolo[5,4-c]pyridine (800 mg) in tetrahydrofuran (24 ml) at room temperature, and the mixture was stirred for 10 minutes. The reaction mixture was concentrated under reduced pressure to obtain the title compound (825 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935824B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-2f802f0b52c14f7489a4d93dc4d06641 |
| Source note | uspto-grants-2011_05 |