HCID 57585939, compound → HCID 57585835, compound

Participants

Reaction Steps

4-{[2-Chloro-4-(1,3-dioxolan-2-yl)phenyl]oxy}-2-nitroaniline (1.41 g) was dissolved in 100 mL of ethyl acetate and hydrogenated over 100 mg of 10% Pd/carbon (wet, Degussa type) under balloon of H2 gas. After 24 hours, the reaction was filtered through Celite and concentrated to give 4-{[2-chloro-4-(1,3-dioxolan-2-yl)phenyl]oxy}-1,2-benzenediamine which was used without further purification. (M+1) 306.9, 1.57 min (LC/MS method B)

Provenance & Evidence