HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9865354, compound → HCID 22319132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9865354 | HCID 9865354 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22319132 | HCID 22319132 | 67.7% |
Reaction Steps
3-(2-Cyanophenyl)-5-(2-nitrophenyl)-1-phenyl-1,2-dihydropyridin-2-one (32 mg) was dissolved in 15 ml of ethyl acetate, 5 mg of 10% palladium-carbon (water-containing substance) were added and the mixture was stirred at room temperature in a hydrogen atmosphere for 15 minutes. The catalyst was filtered off and the solvent was evaporated in vacuo to give 20 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07939549B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-4d2c9b7908174b8dbb6b92d376a8e411 |
| Source note | uspto-grants-2011_05 |