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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 547699Generated: October 31, 2026

Acetic Anhydride → HCID 10159178, compound

https://huagongshe.com/reaction/547699

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 22318959HCID 22318959—
SolventPyridineHCID 1049—
ProductHCID 10159178HCID 10159178—

Reaction Steps

To 56 mg of 3-(2-cyanophenyl)-5-(2-pyridyl)-1-(3-hydroxyphenyl)-1,2-dihydropyridin-2-one were added 1 ml of acetic anhydride and 1 ml of pyridine and the mixture was stirred at room temperature for one night. The reaction solution was concentrated in vacuo and purified by an NH silica gel chromatography (hexane-ethyl acetate system) to give 30 mg of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07939549B2
Source datasetuspto-grants-2011_05
ORD IDord-e9286a54e50442f0b1dcdc9789981ddf
Source noteuspto-grants-2011_05