HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium ethanethioate → Ethanethioic acid trans-(+/-)-S-[5-[[(4-fluorophenyl)sulfonyl]methyl]tetrahydro-3-furanyl]ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium ethanethioate | HCID 23670855 | — |
| Reactant | cis-(+/-)-4-Bromo-2-[[(4-fluorophenyl)sulfonyl]methyl]tetrahydrofuran | HCID 86750318 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Ethanethioic acid trans-(+/-)-S-[5-[[(4-fluorophenyl)sulfonyl]methyl]tetrahydro-3-furanyl]ester | HCID 86750317 | 55.8% |
Reaction Steps
The title compound is prepared by the procedure of Example 5 using 0.969 g of product from Example 30, 0.360 g of potassium thioacetate, and 9 ml of acetonitrile to give 0.533 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05623081 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-e9fde5dbddf24aa187440e8f06f25743 |
| Source note | uspto-grants-1997_04 |