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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 54779Generated: October 25, 2026

Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester → cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol

https://huagongshe.com/reaction/54779

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]esterHCID 86750331—
SolventTetrahydrofuranHCID 8028—
SolventSodium methanolate methanolHCID 23694274—
Productcis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiolHCID 8675033264.8%

Reaction Steps

The title compound is prepared by the procedure of Example 16 using 0.310 g of product from Example 61 in 4.5 ml of tetrahydrofuran and 0.30 ml of sodium methoxide/methyl alcohol to give 0.159 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05623081
Source datasetuspto-grants-1997_04
ORD IDord-6d5cb41560274ce28dc5b3f7aa3ce5be
Source noteuspto-grants-1997_04