HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Amino-3-methyl-butyl)-3-methyl-1,3-dihydro-benzimidazol-2-one → 8-[2-[1,1-dimethyl-3-(3-methyl-2-oxo-2,3-dihydro-benzimidazol-1-yl)-propylamino]-1-hydroxy-ethyl]-6-hydroxy-4H-benzo[1,4]oxazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Amino-3-methyl-butyl)-3-methyl-1,3-dihydro-benzimidazol-2-one | HCID 13174716 | — |
| Reactant | 6-benzyloxy-8-(2-ethoxy-1,2-dihydroxy-ethyl)-4H-benzo[1,4]oxazin-3-one | HCID 67188030 | — |
| Product | 8-[2-[1,1-dimethyl-3-(3-methyl-2-oxo-2,3-dihydro-benzimidazol-1-yl)-propylamino]-1-hydroxy-ethyl]-6-hydroxy-4H-benzo[1,4]oxazin-3-one | HCID 59796442 | — |
Reaction Steps
Prepared according to General Method 2 from 357 mg (1 mmol) 6-benzyloxy-8-(2-ethoxy-1,2-dihydroxy-ethyl)-4H-benzo[1,4]oxazin-3-one and 233 mg (1 mmol) 1-(3-amino-3-methyl-butyl)-3-methyl-1,3-dihydro-benzimidazol-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07939658B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-695747cf10dd465cbbe3d58ffa4f8c0c |
| Source note | uspto-grants-2011_05 |