HRID54792

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID887

Methanol

CH4O

HCID14798

Sodium Hydroxide

HNaO

结构：CC(=O)S[C@H]1CO[C@@H](C(=O)N2CCN(C(=O)OCc3ccc([N+](=O)[O-])cc3)CC2)C1

HCID131719859

未命名化合物

PRODUCTS

生成物

结构：O=C(OCc1ccc([N+](=O)[O-])cc1)N1CCN(C(=O)[C@H]2C[C@@H](S)CO2)CC1

HCID131719858

未命名化合物

收率 41.4%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 153 using 0.230 g of product from Example 157, 0.29 ml of 4N sodium hydroxide and 1.7 ml of methyl alcohol to give 0.086 g of the desired product after chromatography (silica gel: 10 -100% ethyl acetate/hexane).