HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → 3-Butoxy-4-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | 3-Ethoxy-4-methylbenzaldehyde | HCID 25242058 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-Butoxy-4-methoxybenzaldehyde | HCID 592471 | — |
Reaction Steps
The title compound was prepared analogously to 3-ethoxy-4-methyl-benzaldehyde (intermediate B21, vide infra) by reaction of 3-hydroxy-4-methoxy-benzaldehyde with 4-bromo-butane in DMF using K2CO3 as base. MS (ISP): 209.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07939661B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-d2e0ba3f0bb943cca19c67ac2b5f7f30 |
| Source note | uspto-grants-2011_05 |