3-Cyanobenzoic acid → HCID 57944982, compound

HRID 548014Notes

Reaction equation

HRID 548014 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6]([OH:8])=O)#[N:2].Cl.[CH3:13][C:14]1[C:18]([CH2:19][N:20]2[CH:24]=[C:23]([NH2:25])[CH:22]=[N:21]2)=[C:17]([CH3:26])[O:16][N:15]=1>>[C:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6]([NH:25][C:23]1[CH:22]=[N:21][N:20]([CH2:19][C:18]2[C:14]([CH3:13])=[N:15][O:16][C:17]=2[CH3:26])[CH:24]=1)=[O:8])#[N:2]

Participants

3

Reactant 2

HCID 158753-Cyanobenzoic acidHCID 574222641-((3,5-dimethylisoxazol-4-yl)methyl)-1H-pyrazol-4-amine hydrochloride

Product 1

HCID 57944982HCID 57944982, compoundYield 15%

Procedure

Prepared as in Example 4-8 from 3-cyanobenzoic acid and 1-((3,5-dimethylisoxazol-4-yl)methyl)-1H-pyrazol-4-amine hydrochloride (Example 4-1a). Yield 15%. MS M+H calculated 322.6, found 322.3.

Sources & evidence

ORD record
ord-c88276057e03473b9df16668c5a4a61b
Source dataset
uspto-grants-2011_05
Patent number
US07939671B2

Reaction notes

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