HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → N'-(3-Chlorophenyl)-N,N-dimethylmethanimidamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | N'-(3-Chlorophenyl)-N,N-dimethylmethanimidamide | HCID 415383 | 100.5% |
Reaction Steps
A mixture of 3-chloroaniline (63.8 g, 0.50 mol) and dimethylformamide dimethyl acetal (106 ml, 0.75 mol) was heated at 100° for 2 h and evaporated at 60° at 0.5 mm Hg to give 91.8 g amber oil; ms 183.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE042376E1 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-39ce25f3d8bb4aeda4ce9dd1583f6e98 |
| Source note | uspto-grants-2011_05 |