3,4,5-Trifluorophenol → HCID 178447737, compound

HRID 54877Notes

Reaction equation

HRID 54877 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([F:9])[C:7]=1[F:8].[C:11]1([Si:17]2(CCCCC)[CH2:22][CH2:21][CH:20]([C:23]3[CH:31]=[CH:30][C:26]([C:27](O)=[O:28])=[CH:25][CH:24]=3)[CH2:19][CH2:18]2)C=[CH:15][CH:14]=[CH:13][CH:12]=1>>[CH2:11]([Si@H:17]1[CH2:18][CH2:19][C@H:20]([C:23]2[CH:31]=[CH:30][C:26]([C:27]([O:10][C:4]3[CH:3]=[C:2]([F:1])[C:7]([F:8])=[C:6]([F:9])[CH:5]=3)=[O:28])=[CH:25][CH:24]=2)[CH2:21][CH2:22]1)[CH2:12][CH2:13][CH2:14][CH3:15]

Participants

3

Reactant 2

HCID 27779433,4,5-TrifluorophenolHCID 199567094-(4-Phenyl-4-n-pentyl-4-silacyclohexyl)benzoic acid

Product 1

HCID 178447737HCID 178447737, compound

Procedure

The general procedure of Example 3 was repeated using 3,4,5-trifluorophenol and 4-(4-phenyl-4-n-pentyl-4-silacyclohexyl)benzoic acid, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-e69dd5f7a54a4a5caa414d8ac3392e56
Source dataset
uspto-grants-1997_04
Patent number
US05624601

Reaction notes

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