HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 42629890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 6-(5-Methyl-3-phenyl-isoxazol-4-ylmethoxy)-pyridazin-3-ylamine | HCID 42629771 | — |
| Product | HCID 42629890 | HCID 42629890 | 65% |
Reaction Steps
As described for example 18, 6-(5-methyl-3-phenyl-isoxazol-4-ylmethoxy)-pyridazin-3-ylamine (280 mg, 1 mmol) was converted, using benzoyl chloride instead of methoxyacetyl chloride, to the title compound (250 mg, 65%) which was obtained as a white solid. MS: m/e=387.4 [M+H]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943619B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-a9663a832aa645efa9359ccaf87fe968 |
| Source note | uspto-grants-2011_05 |