HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1,2-dichlorobenzene → 3-(3,4-Dichlorophenyl)-9-methyl-3,9-diazaspiro[5.5]undecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1,2-dichlorobenzene | HCID 29013 | — |
| Reactant | 3-Methyl-3,9-diazaspiro[5.5]undecane | HCID 21813293 | — |
| Product | 3-(3,4-Dichlorophenyl)-9-methyl-3,9-diazaspiro[5.5]undecane | HCID 15940644 | — |
Reaction Steps
Was prepared according to method A from 3-methyl-3,9-diaza-spiro[5.5]undecane and 1-bromo-3,4-dichlorobenzene as a yellow oil. LC-ESI−HRMS of [M+H]+ shows 313.1238 Da. Calc. 313.123829 Da, dev. −0.1 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943630B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-8adc561014414367a43e66ed6c2e86fe |
| Source note | uspto-grants-2011_05 |