反应详情

温度

200 °C

3-chlorophenyl acetate (starting material 2) was mixed with aluminium chloride (3 eq). The mixture was heated at 200° C. for 1 hour. The reaction medium was cooled to room temperature then poured in ice. The aqueous phase was extracted with methylene chloride which was dried on magnesium sulfate then vacuum evaporated.

1. temperatureThe reaction medium was cooled to room temperature
2. additionthen poured in ice
3. extractionThe aqueous phase was extracted with methylene chloride which
4. customwas dried on magnesium sulfate
5. customvacuum evaporated