HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178477906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178452256 | HCID 178452256 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178477906 | HCID 178477906 | — |
Reaction Steps
TFA (2 mL) was added to a solution of tert-butyl 4-(5-chloro-1H-benzimidazol-2-yl)piperazine-1-carboxylate (72 mg) in DCM (2 mL) and the reaction was stirred for 1 h. The solvent was then evaporated under high vacuum for 1 h to afford the title compound as a gum which was used without further analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943768B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-35bbc3851f544ae092e4cdeb7b05263c |
| Source note | uspto-grants-2011_05 |