HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Diisobutyl aluminium azide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | Diisobutyl aluminium azide | HCID 86610998 | — |
Reaction Steps
1.235 g of granular sodium azide (19 mmol) are added to a cold solution of dilsobutyl aluminium chloride (19 mmol, 1.8M in toluene) diluted in 5 ml of toluene and the mixture is stirred at room temperature over the night to give diisobutyl aluminium azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943647B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-6553c153fbc1461bb6dcfc66c7c1b8bd |
| Source note | uspto-grants-2011_05 |