反应详情

温度

32 °C

Into the flask described hereinabove there were placed 204.2 grams of aluminium tri-isopropanolate to which 216 grams of acrylic acid were added during 8 minutes at room temperature (25° C.). The procedure was as set forth hereinabove. Owing to the reaction heat, the temperature increased to 32° C. The resultant product was a white, solid substance. The rotary evaporator heating then was switched on and gradually heated to 70° C. At the same time the vacuum was gradually adjusted to 24 mbar. The isopropanol was thereby expelled yielding a white powder.

1. additionwere added during 8 minutes at room temperature (25° C.)
2. temperatureOwing to the reaction heat
3. customThe rotary evaporator
4. temperatureheating
5. temperaturegradually heated to 70° C
6. customThe isopropanol was thereby expelled yielding a white powder