Hydrochloric Acid → HCID 66631176, compound

Participants

Reaction Steps

Using an analogous procedure to that described in Example 36, N-{5-[(cyclopropylamino)carbonyl]-2-methylphenyl}-3-fluoro-4-(pyridin-2-ylmethoxy)benzamide was reacted with hydrochloric acid to give the title compound; NMR Spectrum: (DMSOd6) 0.57 (m, 2H), 0.68 (m, 2H), 2.28 (s, 3H), 2.86 (m, 1H), 5.60 (s, 2H), 7.32 (m, 1H), 7.43 (m, 1H), 7.66 (m, 1H), 7.84 (m, 5H), 8.40 (m, 2H), 8.83 (m, 1H), 10.07 (br s, 1H); Mass Spectrum: M+H+ 420.

Provenance & Evidence