HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57871412, compound → HCID 57871415, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57871412 | HCID 57871412 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57871415 | HCID 57871415 | 94% |
Reaction Steps
Treat a mixture of 3-(7-benzyloxynaphthalen-2-yl)pentan-3-ol (1.45 g, 4.53 mmol) and 5% Pd/Al2CO3 (0.044 g) in EtOH (725 mL) with hydrogen at 60 psi for 8 h at RT. Remove the catalyst by filtration and concentrate the filtrate to give the title compound as a yellow oil (0.98 g, 94%). MS (ES) m/e 229 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943795B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-779e5e65fb034541b4675fda3001258d |
| Source note | uspto-grants-2011_05 |