HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 67199887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Pyridine, 4-(4-dimethylaminophenyl)- | HCID 227783 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67199887 | HCID 67199887 | 18% |
Reaction Steps
IDT321. Was prepared by refluxing N,N-dimethyl-4-(pyridine-4-yl) aniline (II) in acetonitrile in the presence of ethyl iodide. Upon cooling diethyl ether was added and the product crystallized resulting in a 18% yield of 4-(4-(dimethylamino)phenyl)-1-ethylpyridinium iodide (IDT321) (IV).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947255B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-8ac69fa2f8b74e39863302a8ef815c00 |
| Source note | uspto-grants-2011_05 |