HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Glucosamine → D-glucosamine 5-methyl-(6R,S)-tetrahydrofolate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Glucosamine | HCID 439213 | — |
| Reactant | (6r,s)-5-Methyltetrahydrofolic acid | HCID 135430866 | — |
| Product | D-glucosamine 5-methyl-(6R,S)-tetrahydrofolate | HCID 136356796 | 132.5% |
Reaction Steps
9.19 g (20 mmol) of 5-methyl-(6R,S)-tetrahydrofolic acid were added portion-wise and completely dissolved in 60 ml of an aqueous solution of D-glucosamine (7.12 g, 40 mmol) stirred under nitrogen. The resulting solution (pH 6.53) was spray-dried, obtaining 16.9 g of the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947662B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-84673e28f0b3451798c24b28fa0f8bb4 |
| Source note | uspto-grants-2011_05 |