反应详情

Sodium azide (22.8, 0.351 mol) in water (60 mL) was added to a solution of 2-(2-bromoethyl)-nitrobenzene (27.9 g, 0.121 mol) in acetonitrile (120 mL). The reaction was refluxed for 4 h, cooled, and partitioned between methylene chloride and water. The organic phase was washed with saturated brine, and dried over magnesium sulfate. The title compound was obtained as an oil (22.8 g).

1. temperatureThe reaction was refluxed for 4 h
2. temperaturecooled
3. custompartitioned between methylene chloride and water
4. washThe organic phase was washed with saturated brine
5. dry with materialdried over magnesium sulfate