HCID 17950069, compound → HCID 11647266, compound

Participants

Reaction Steps

The procedure described in Example 1 was repeated using N′-[4-cyano-3-(2-hydroxyethoxy)-1H-pyrazol-5-yl]-N,N-dimethylimidoformamide (800 mg, 3.58 mmol) and 3-chloro-4-[(6-methylpyridin-3-yl)oxy]aniline (925 mg, 3.94 mmol) to give the title compound as a white solid (770 mg, 52%); NMR Spectrum: 2.45 (s, 3H), 3.81 (br t, 2H), 4.34 (t, 2H), 5.13 (br s, 1H), 7.21 (d, 1H), 7.26 (s, 1H), 7.27 (s, 1H), 7.71 (dd, 1H), 8.10 (d, 1H) 8.21 (s, 1H), 8.34 (s, 1H), 8.62 (br s, 1H); Mass Spectrum: 413 (MH+).

Provenance & Evidence