HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethylthiazole-5-carbohydrazide → 4-methyl-3-(4-methyl-1,3-thiazol-5-yl)-5-(4-penten-1-yl)-4H-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethylthiazole-5-carbohydrazide | HCID 2743669 | — |
| Reactant | N,N'-dimethyl-5-hexenimidamide hydrochloride | HCID 86630240 | — |
| Product | 4-methyl-3-(4-methyl-1,3-thiazol-5-yl)-5-(4-penten-1-yl)-4H-1,2,4-triazole | HCID 57691885 | — |
Reaction Steps
The title compound was prepared in analogy to Preparation 11 in 0.31 g yield starting from 2,4-dimethyl-thiazole-5-carboxylic acid hydrazide (0.52 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.58 g). MS (m/z): 249 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947683B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-a69be5f9d8f2491fb78534d8907da9cf |
| Source note | uspto-grants-2011_05 |