3-Chlorobenzohydrazide → HCID 57691934, compound

HRID 550542Notes

Reaction equation

HRID 550542 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][CH:11]=1)[C:5]([NH:7][NH2:8])=O.Cl.[CH3:13][NH:14][C:15](=NC)[CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20]>>[Cl:1][C:2]1[CH:3]=[C:4]([C:5]2[N:14]([CH3:13])[C:15]([CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20])=[N:8][N:7]=2)[CH:9]=[CH:10][CH:11]=1

Participants

3

Reactant 2

HCID 742893-ChlorobenzohydrazideHCID 86630240N,N'-dimethyl-5-hexenimidamide hydrochloride

Product 1

HCID 57691934HCID 57691934, compound

Procedure

The title compound was prepared in analogy to Preparation 11 in 0.16 g yield starting from 3-chlorobenzhydrazide (0.52 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.48 g). MS (m/z): 262 [MH]+.

Workup

  1. customyield

Sources & evidence

ORD record
ord-849a4aa19f1e43e5bf7de15b8d12785d
Source dataset
uspto-grants-2011_05
Patent number
US07947683B2

Reaction notes

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