Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene → 1-[4-(2-Quinolyl)thiophenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene | HCID 520026 | — |
| 반응물 | 2-(4-Aminophenylthio)quinoline | HCID 22637130 | — |
| 생성물 | 1-[4-(2-Quinolyl)thiophenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea | HCID 9957209 | 56% |
반응 단계
2-(4-aminophenylthio) quinoline (3.9 mmoles, 1.0 g) and 4-chloro-3 -trifluoromethylphenylisothiocyanate (3.9 mmoles, 0.92 g) were reacted according to procedure A to yield 1.06 g, 56% of the title compound. Mass spec (FD) 490. Calculated for C23H15ClF3N3S2 : C, 56.38; H, 3.09, N, 8.58. Found: C, 56.60; H, 3.11; N, 8.42.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05624937 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-0aff014633c84a4fa3a186008eecaf7a |
| 출처 메모 | uspto-grants-1997_04 |