HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene → 1-[4-(4-Phenyl-2-quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene | HCID 520026 | — |
| Edukt | 2-(4-Aminophenylthio)-4-phenylquinoline | HCID 18971678 | — |
| Produkt | 1-[4-(4-Phenyl-2-quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea | HCID 18971679 | 61% |
Reaktionsschritte
2-(4-aminophenylthio)-4-phenylquinoline (3.0 moles, 1.0 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (3.3 mmoles, 0.79 g) were reacted according to procedure C to yield the title compound 1.03 g, 61%. Mass Spec (FD) 565. Calculated for C29H19ClF3N3S2 : C, 61.53; H, 3.38; N, 7.42. Found: C, 61.82; H, 3.63; N, 7.43.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05624937 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-99b53dac1188446eba3c92c87c24075b |
| Quellennotiz | uspto-grants-1997_04 |