HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetylphenylboronic acid → HCID 59846303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetylphenylboronic acid | HCID 3702122 | — |
| Reactant | HCID 11704093 | HCID 11704093 | — |
| Product | HCID 59846303 | HCID 59846303 | — |
Reaction Steps
1-(4-Bromo-benzyl)-3-hydroxy-1H-benzo[4,5]thieno[3,2-d]pyrimidine-2,4-dione was treated with 4-acetylphenylboronic acid according to general procedure C. The title compound was obtained as a yellow solid following purification by preparative HPLC. 1H NMR (d6-DMSO, 300 MHz) δ 2.63 (s, 3H); 5.80 (s, 2H); 7.70-8.20 (m, 12H); Ret. time=2.89, m/z=441.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947691B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-de5966e0d1104208ae86f05ddd0d26ca |
| Source note | uspto-grants-2011_05 |