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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 550734Generated: October 30, 2026

4-Acetylphenylboronic acid → HCID 59846303, compound

https://huagongshe.com/reaction/550734

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Acetylphenylboronic acidHCID 3702122—
ReactantHCID 11704093HCID 11704093—
ProductHCID 59846303HCID 59846303—

Reaction Steps

1-(4-Bromo-benzyl)-3-hydroxy-1H-benzo[4,5]thieno[3,2-d]pyrimidine-2,4-dione was treated with 4-acetylphenylboronic acid according to general procedure C. The title compound was obtained as a yellow solid following purification by preparative HPLC. 1H NMR (d6-DMSO, 300 MHz) δ 2.63 (s, 3H); 5.80 (s, 2H); 7.70-8.20 (m, 12H); Ret. time=2.89, m/z=441.0.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07947691B2
Source datasetuspto-grants-2011_05
ORD IDord-de5966e0d1104208ae86f05ddd0d26ca
Source noteuspto-grants-2011_05