1-(Bromomethyl)-2-phenylbenzene → HCID 11510580, compound

Participants

Reaction Steps

Following general procedure B2 and D1, 3-(2,4-Dimethoxy-benzyloxy)-8-nitro-1H-benzo[4,5]thieno[3,2-d]pyrimidine-2,4-dione was alkylated with 2-phenylbenzyl bromide and subsequently deprotected to provide the title compound as a light yellow solid. 1H NMR (d6-DMSO, 300 MHz) δ 5.53 (s, 2H); 7.20-7.57 (m, 9H); 8.29 (dd, J1=9 Hz, J2=2 Hz, 1H); 8.36 (d, J=2 Hz, 1H); 8.40 (d, J=9 Hz, 1H); Ret. time=3.14 min., m/z=444.0.

Provenance & Evidence