1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene → 1-[4-(2-Naphthylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene	HCID 520026	—
Edukt	2-(4-Aminophenylthio)naphthalene	HCID 18971645	—
Produkt	1-[4-(2-Naphthylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea	HCID 18971665	34,1%

Reaktionsschritte

2-(4-Aminophenylthio)naphthalene (4.2 mmoles, 1.06 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (4.2 mmoles, 0.93 g) were reacted according to procedure A to yield of the title compound 0.7 g, 34%. Mass Spec (FD) 489. Calculated for C24H16ClF3N2S2 : C,; H, N, Found: C,; H,; N,.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US05624937
Quelldatensatz	uspto-grants-1997_04
ORD ID	ord-2843050ee8f5474a8d8861a0839108f2
Quellennotiz	uspto-grants-1997_04