HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → 2-(4-Aminophenylthio)naphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-(4-Nitrophenylthio)naphthalene | HCID 18971685 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(4-Aminophenylthio)naphthalene | HCID 18971645 | 47% |
Reaction Steps
2-(4-nitrophenylthio)naphthalene (9.2 moles, 2.6 g) was dissolved in 50 ml ethanol and 20 ml ethyl acetate and hydrogenated for 16 hrs at room temperature over 1.0 g 5% Pd/C. The solution was filtered through celite and concentrated to yield 2-(4-aminophenylthio)naphthalene 1.1 g, 47%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05624937 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-2d5e005bea104a578197412c06cc98bd |
| Source note | uspto-grants-1997_04 |