HRID55081

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID520026

4-Chloro-3-(trifluoromethyl)phenyl isothiocyanate

C8H3ClF3NS

HCID13718379

未命名化合物

PRODUCTS

生成物

结构：FC(F)(F)c1cc(NC(=S)Nc2ccc(Sc3nc4ccccc4o3)cc2)ccc1Cl

HCID18971648

未命名化合物

收率 33%

PROCEDURE

实验过程

2-(4-Aminophenylthio)benzoxazole (10.0 moles, 2.6 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (10.0 moles, 2.4 g) were reacted according to procedure A to yield of the title compound 1.6 g, 33%. Mass Spec (FD) 479. Calculated for C21H13ClF3N3OS2 : C, 52.56; H, 2.73; N, 8.75. Found: C, 52.47; H, 2.70; N, 8.48.