HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(2-benzyloxy-ethoxy)-propionate → Ethyl 3-(2-hydroxyethoxy)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(2-benzyloxy-ethoxy)-propionate | HCID 66731906 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(2-hydroxyethoxy)propanoate | HCID 22394031 | — |
Reaction Steps
3.73 g (14.8 mmol) ethyl 3-(2-benzyloxy-ethoxy)-propionate are hydrogenated together with 665 mg 10% palladium charcoal in 70 ml of ethanol for 44 minutes at ambient temperature under a hydrogen atmosphere at 3 bar. Then the mixture is suction filtered and the filtrate is evaporated down i. vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947700B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-3705c9c3a89048f8b0fcbda67a26d345 |
| Source note | uspto-grants-2011_05 |