HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 57349451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | (6-Methoxypyridin-3-yl)boronic acid--hydrogen chloride (1/1) | HCID 22309456 | — |
| Reactant | HCID 86761320 | HCID 86761320 | — |
| Product | HCID 57349451 | HCID 57349451 | — |
Reaction Steps
The title compound is prepared as described in EXAMPLE 31, Part I, but with 6-bromonicotinic acid hydrochloride and 6-methoxypyridin-3-ylboronic acid hydrochloride as starting materials, and 10 molar equivalents of 0.4M aqueous sodium carbonate. 1H NMR (DMSO) δ 13.40 (br s, 1H), 9.10 (d, 1H), 8.95 (d, 1H), 8.43 (dd, 1H), 8.28 (dd, 1H), 8.09 (d, 1H), 6.95 (d, 1H), 3.91 (s, 3H). ESI MS (M+1)+: 231.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947684B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-c26bd520b62645e88c0cf3fe277d8a80 |
| Source note | uspto-grants-2011_05 |