HCID 67196591, compound → HCID 67192481, compound

Participants

Reaction Steps

The title compound is prepared as described in EXAMPLE 44, parts A and B, but with 6′-oxo-1′,6′-dihydro-[2,3′]bipyridinyl-5-carboxylic acid, and 5-[4-(4-chloro-1H-pyrrolo[3,2-c]pyridin-2-yl)piperidine-1-carbonyl]-1′H-[2,3′]bipyridinyl-6′-one trifluoroacetate as starting materials, respectively. 1H NMR (d4-MeOH) δ 8.67-8.65 (m, 1H), 8.32 (dd, 1H), 8.25 (d, 1H), 7.92 (dd, 1H), 7.85 (dd, 1H), 7.40 (d, 1H), 6.94 (d, 1H), 6.68-6.63 (m, 2H), 4.85-4.70 (m, 1H), 3.99-3.82 (m, 1H), 3.42-3.03 (m, 3H), 2.24-2.06 (m, 2H), 1.88-1.68 (m, 2H). ESI MS (M+1)+: 415.

Provenance & Evidence