4-methylnaphthalen-1-amine → HCID 59763695, compound

HRID 551365Notes

Reaction equation

HRID 551365 reaction equation
CC1C2C(=CC=CC=2)C(N)=CC=1.[CH2:13]([C:15]1[CH:24]=[CH:23][C:22]([N+:25]([O-])=O)=[C:21]2[C:16]=1[CH2:17][CH2:18][CH2:19][CH2:20]2)[CH3:14]>>[CH2:13]([C:15]1[C:16]2[CH2:17][CH2:18][CH2:19][CH2:20][C:21]=2[C:22]([NH2:25])=[CH:23][CH:24]=1)[CH3:14]

Participants

3

Reactant 2

HCID 4311874-methylnaphthalen-1-amineHCID 66632821HCID 66632821, compound

Product 1

HCID 59763695HCID 59763695, compound

Procedure

The procedure was essentially identical to the route for 4-Methyl-naphthalen-1-ylamine as described above, however, started with a solution of 5-ethyl-8-nitro-1,2,3,4-tetrahydro-naphthalene (795 mg, 3.95 mmol).

Sources & evidence

ORD record
ord-1e1d94328ee040e2a2bb370c0b7adc47
Source dataset
uspto-grants-2011_05
Patent number
US07947721B2

Reaction notes

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