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Thionyl Chloride → 4-[(2-methylbenzoyl)amino]benzoyl Chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 4-[(2-methylbenzoyl)amino]benzoic Acid | HCID 11615814 | — |
| 生成物 | 4-[(2-methylbenzoyl)amino]benzoyl Chloride | HCID 10707441 | — |
反応手順
A mixture of 10.3 g of 4-[(2-methylbenzoyl)amino]benzoic acid and 32 ml of thionyl chloride is refluxed for 1.5 hours. The solution is concentrated in vacuo. Toluene is added and the solvent removed in vacuo. Toluene is added and the mixture chilled and filtered to give the desired product as a yellow solid, 135°-141° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05624923 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-08bfdbd7ef204255a26d113231fd2242 |
| 出典メモ | uspto-grants-1997_04 |