(5-Bromo-3-pyridinyl)methanol → HCID 11702341, compound

Participants

Reaction Steps

5-Bromo-pyridine-3-carbaldehyde. (5-Bromo-pyridin-3-yl)-methanol (1.13 g, 6.00 mmol) was dissolved in CHCl3 (40 mL) and treated with MnO2 (3.60 g). The reaction mixture was heated at reflux temperature for 3 h. The hot reaction mixture was filtered through a pad of diatomaceous earth and the filtrate was concentrated to yield the title compound (0.570 g, 51%).

Provenance & Evidence