HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 86646155, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 3-(Prop-2-en-1-yl)oxolan-2-ol | HCID 13545767 | — |
| Reactant | HCID 178473672 | HCID 178473672 | — |
| Product | HCID 86646155 | HCID 86646155 | — |
Reaction Steps
3-allyl-tetrahydrofuran-2-ol (18 g, 140 mmol) and ethoxycarbonyl triphenylphosphorane (35 g, 104 mmol) were stirred overnight in toluene (200 mL). The reaction solution was concentrated, and the residue was purified by silica gel column chromatography to obtain the compound of interest as an oil substance (15.8 g, 61.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947738B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-27af5f9a4e42434abf0c6c363f642844 |
| Source note | uspto-grants-2011_05 |