HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-1,3-propanediamine → HCID 86615836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | Sodium Sulfate | HCID 24436 | — |
| Reactant | HCID 51050327 | HCID 51050327 | — |
| Product | HCID 86615836 | HCID 86615836 | 89% |
Reaction Steps
In a procedure analogously to 2,2-dimethyl-5-(dimethylaminoethyl-imino)-3-hexanone, starting with 2,2-dimethylhexa-3,5-dione (19.27 g, 136 mmol), Na2SO4 (13 g, 92 mmol), and 3-(dimethylamino)propylamine (15.72 g, 154 mmol). A yellow liquid was obtained via a short-path vacuum distillation apparatus after removal of all volatiles. The yield is 89%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947814B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-1299c17f488d4fb1a55b248ad4a9b3b0 |
| Source note | uspto-grants-2011_05 |