HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Sulfate → 4-[[2-(Dimethylamino)ethyl]imino]-2-pentanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Sulfate | HCID 24436 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | HCID 51050327 | HCID 51050327 | — |
| Product | 4-[[2-(Dimethylamino)ethyl]imino]-2-pentanone | HCID 13677035 | 83% |
Reaction Steps
In a procedure analogously to 2,2-dimethyl-5-(dimethylaminoethyl-imino)-3-hexanone, starting with starting with 2,4-pentadione (8.00 g, 80.7 mmol), Na2SO4 (14 g, 98.64 mmol), and 3-(dimethylamino)ethylamine (7.83 g, 88.8 mmol). A green liquid was obtained via vacuum distillation at an oil bath of 95-105° C. under 150 mTorr. The yield was 83%. GC analysis indicated one peak.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947814B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-8f040cee56884149b97671938eb19193 |
| Source note | uspto-grants-2011_05 |