HRID551790

反应详情

EQUATION

反应方程式

HRID 551790 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

13.3 g of 1-(1H-imidazol-1-ylcarbonyl)-1,2,3,4-tetrahydroquinoline, 133 ml of acetonitrile and 14.6 ml of iodomethane are introduced into a 500 ml round-bottomed flask. The reaction mixture is stirred for 20 h and then the solvent is evaporated under reduced pressure to result in 23 g of 1-(3,4-dihydroquinolin-1(2H)-ylcarbonyl)-3-methyl-1H-imidazol-3-ium iodide.

WORKUP

后处理

  1. customthe solvent is evaporated under reduced pressure
  2. customto result in 23 g of 1-(3,4-dihydroquinolin-1(2H)-ylcarbonyl)-3-methyl-1H-imidazol-3-ium iodide