HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Hydroxyphthalimide → HCID 10892514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | HCID 10935615 | HCID 10935615 | — |
| Product | HCID 10892514 | HCID 10892514 | 53% |
Reaction Steps
3β-methoxyandrost-5-ene-17β-ol (27) was subjected to air oxidation in the presence of N-hydroxyphthalimide and the producT 3β-methoxy-17β-hydroxyandrost-5-ene-7-one (28) was obtained in 53% yield. An analytical sample was obtained by recrystallization from acetone-hexane, m.p. 202-4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947846B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-429bcc78b85e4c2eb8a93fc5028e6748 |
| Source note | uspto-grants-2011_05 |